Crystallization Kinetics of Precisely Synthesized Discrete Oligo(<italic style="font-style: italic">γ</italic>-butyrolactone)s

Ao Feng; Su-hua Duan; Xiao-huan Cao; Rui Tan; Zhi-hao Huang; Xiao-hua Zhang; Zheng-biao Zhang

doi:10.11777/j.issn1000-3304.2022.22150

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Crystallization Kinetics of Precisely Synthesized Discrete Oligo(γ-butyrolactone)s

Research Article | 更新时间：2024-10-08

- Crystallization Kinetics of Precisely Synthesized Discrete Oligo(γ-butyrolactone)s
  增强出版
- ACTA POLYMERICA SINICA Vol. 53, Issue 9, Pages: 1131-1141(2022)
- 作者机构：
  
  1.苏州大学材料与化学化工学部苏州 215123
  2.苏州大学软凝聚态物理及交叉研究中心
  3.苏州大学物理科学与技术学院苏州 215006
- 作者简介：
  
  Zhi-hao Huang, E-mail: zhhuang@suda.edu.cn
  Xiao-hua Zhang, E-mail: zhangxiaohua@suda.edu.cn
  Zheng-biao Zhang, E-mail: zhangzhengbiao@suda.edu.cn
- 基金信息：
- DOI：10.11777/j.issn1000-3304.2022.22150
  CLC：
- Published：20 September 2022，
  
  Published Online：12 July 2022，
  
  Received：27 April 2022，
  
  Accepted：07 June 2022
- 稿件说明：
移动端阅览
冯澳,段素华,曹晓环等.单一分子量γ-丁内酯齐聚物的合成及其结晶行为研究[J].高分子学报,2022,53(09):1131-1141.

Feng Ao,Duan Su-hua,Cao Xiao-huan,et al.Crystallization Kinetics of Precisely Synthesized Discrete Oligo(γ-butyrolactone)s[J].ACTA POLYMERICA SINICA,2022,53(09):1131-1141.
冯澳,段素华,曹晓环等.单一分子量γ-丁内酯齐聚物的合成及其结晶行为研究[J].高分子学报,2022,53(09):1131-1141. DOI： 10.11777/j.issn1000-3304.2022.22150.

Feng Ao,Duan Su-hua,Cao Xiao-huan,et al.Crystallization Kinetics of Precisely Synthesized Discrete Oligo(γ-butyrolactone)s[J].ACTA POLYMERICA SINICA,2022,53(09):1131-1141. DOI： 10.11777/j.issn1000-3304.2022.22150.

摘要

聚

-丁内酯作为一种真正意义上可以实现“单体—聚合物—单体”的可循环聚酯种类，其结构性能的精准研究引起了广泛的兴趣. 本文从生物基原料丁内酯和丁二酸酐出发，通过迭代指数级增长策略结合高效的酯化条件，合成了一系列单一分子量

-丁内酯齐聚物，其结构经过了核磁共振氢谱，凝胶渗透色谱和大分子质谱的严格表征，并研究了这些单一分子量

-丁内酯齐聚物的结晶行为. 结果表明，单一分子量

-丁内酯齐聚物的熔融温度随分子量的增加而升高，而多分散样品的熔融温度与分子量近似的单一分子量

-丁内酯齐聚物相似. 在相同结晶温度下，分子量越高，成核速率和球晶生长速率越大，结晶越快. 多分散样品的结晶行为主要受高分子量组分的影响.

Abstract

$.abstracts[1]

关键词

单一分子量高分子γ-丁内酯齐聚物迭代指数及增长结晶行为

Keywords

Discrete polymerOligo(γ-butyrolactone)Iterative exponential growthCrystalline behaviors

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Crystallization Kinetics of Precisely Synthesized Discrete Oligo(γ-butyrolactone)s

DOI：10.11777/j.issn1000-3304.2022.22150

摘要

Abstract

关键词

Keywords

references