SYNTHESIS OF A WELL-DEFINED HAMMER-LIKE C60 CONJUGATED POLY(2-HYDROXYETHYL ACRYLATE) AND ITS SELF-ASSEMBLY IN WATER

LI Chunzhao; ZHANG Weicheng; WEI Liuhe; DU Fusheng; LI Zichen; LI Fumian

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SYNTHESIS OF A WELL-DEFINED HAMMER-LIKE C60 CONJUGATED POLY(2-HYDROXYETHYL ACRYLATE) AND ITS SELF-ASSEMBLY IN WATER

Research Bulletin | 更新时间：2021-03-19

- SYNTHESIS OF A WELL-DEFINED HAMMER-LIKE C60 CONJUGATED POLY(2-HYDROXYETHYL ACRYLATE) AND ITS SELF-ASSEMBLY IN WATER
- Acta Polymerica Sinica Issue 1, Pages: 120-122(2002)
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- Published：20 February 2002，
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LI Chunzhao, ZHANG Weicheng, WEI Liuhe, DU Fusheng, LI Zichen, LI Fumian. SYNTHESIS OF A WELL-DEFINED HAMMER-LIKE C60 CONJUGATED POLY(2-HYDROXYETHYL ACRYLATE) AND ITS SELF-ASSEMBLY IN WATER. [J]. Acta Polymerica Sinica (1):120-122(2002)
DOI：

LI Chunzhao, ZHANG Weicheng, WEI Liuhe, DU Fusheng, LI Zichen, LI Fumian. SYNTHESIS OF A WELL-DEFINED HAMMER-LIKE C60 CONJUGATED POLY(2-HYDROXYETHYL ACRYLATE) AND ITS SELF-ASSEMBLY IN WATER. [J]. Acta Polymerica Sinica (1):120-122(2002) DOI：

摘要

Abstract

Atom transfer radical polymerization of protected 2-hydroxyethyl acrylate (HEA-TMS) was conducted to prepare well-defined bromo-terminated macroinitiators

which were further allowed to react with large excess amount of C60 under ATRP condition．A well-defined hammer-shaped C60-PHEA was then obtained by hydrolysis of C60-PHEA-TMS under mild conditions．A TEM observation of the association behavior of these well-defined hammer-like C60-PHEA macromolecules showed that they assemble into spherical vesicles in water．Their characteristic inner water phase was further confirmed by fluorescence probe method．Also

it was found that the size of vesiclesdecreased as the increase of molecular weight of PHEA．

关键词

原子转移自由基聚合链球型含C60聚合物囊泡透射电镜荧光

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Department of Applied Chemistry,School of Science,Northwestern Polytechnical University

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