SYNTHESIS OF 1,3DIVINYL1,1,3,3TETRAMETHYL DISILOXANE/STYRENE CYCLOCOPOLYMER AND THEIR THERMAL PROPERTIES

WANG Wenjun; SHIN Franklin; CHAN T.C.

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SYNTHESIS OF 1,3DIVINYL1,1,3,3TETRAMETHYL DISILOXANE/STYRENE CYCLOCOPOLYMER AND THEIR THERMAL PROPERTIES

Research Bulletin | 更新时间：2021-03-19

- SYNTHESIS OF 1,3DIVINYL1,1,3,3TETRAMETHYL DISILOXANE/STYRENE CYCLOCOPOLYMER AND THEIR THERMAL PROPERTIES
- Acta Polymerica Sinica Issue 4, Pages: 477-481(1998)
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- Published：20 August 1998，
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WANG Wenjun, SHIN Franklin, CHAN T.C.. SYNTHESIS OF 1,3DIVINYL1,1,3,3TETRAMETHYL DISILOXANE/STYRENE CYCLOCOPOLYMER AND THEIR THERMAL PROPERTIES. [J]. Acta Polymerica Sinica (4):477-481(1998)
DOI：

WANG Wenjun, SHIN Franklin, CHAN T.C.. SYNTHESIS OF 1,3DIVINYL1,1,3,3TETRAMETHYL DISILOXANE/STYRENE CYCLOCOPOLYMER AND THEIR THERMAL PROPERTIES. [J]. Acta Polymerica Sinica (4):477-481(1998) DOI：

摘要

１

３二烯基１

１

３

３四甲基二硅氧烷／苯乙烯共聚物的合成及其热性能王文俊（浙江大学高分子科学与工程研究所杭州３１００２７）ＳＨＩＮＦｒａｎｋｌｉｎＧ．１

２

ＣＨＡＮＴ．Ｃ．１

３（香港理工大学１材料研究中心２应用物理学系３应用生物及化学技术学系九龙红香港关键词１

３二烯基１

１

３

３四甲基二硅氧烷

苯乙烯

环状共聚物

环化共聚合

热性能有机硅聚合物具有柔软、耐热、?...

Abstract

The solution cyclocopolymerization of 1

3divinyl1

3tetramethyldisiloxane (DVDS) with styrene(St)

using dicumy1 peroxide as initiator is reported. The 29Si-NMR spectra indicated that the cyclocopolymers had the fiveand sixmembered ring

saturated acyclic

and unsaturated acyclic structures formed from DVDS. The thermal properties of cyclocopolymer were investigated by DSC and TGA. It showed that the heatresistant properties of St polymer were improved via copolymerizing with DVDS

and the high degradation temperatures existed in the cyclocopolymers having both high molecular weight and DVDS content.

关键词

１.３-二烯基-１.１.３.３-四甲基二硅氧烷苯乙烯环状共聚物环化共聚合热性能

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