STUDY ON THE PREPARATION OF HIGH MOLECULAR WEIGHT POLY(FERROCENYL DIMETHYLSILANE) THROUGH THERMAL RING OPENING POLYMERIZATION AND POLY(FERROCENYLDIMETHYLSILANE)/TCNE CHARGE TRANSFER COMPLEX

WANG Li; PAN Jie; JI Bing; FENG Linxian

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STUDY ON THE PREPARATION OF HIGH MOLECULAR WEIGHT POLY(FERROCENYL DIMETHYLSILANE) THROUGH THERMAL RING OPENING POLYMERIZATION AND POLY(FERROCENYLDIMETHYLSILANE)/TCNE CHARGE TRANSFER COMPLEX

Research Bulletin | 更新时间：2021-03-19

- STUDY ON THE PREPARATION OF HIGH MOLECULAR WEIGHT POLY(FERROCENYL DIMETHYLSILANE) THROUGH THERMAL RING OPENING POLYMERIZATION AND POLY(FERROCENYLDIMETHYLSILANE)/TCNE CHARGE TRANSFER COMPLEX
- Acta Polymerica Sinica Issue 6, Pages: 788-790(2000)
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- Published：20 December 2000，
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WANG Li, PAN Jie, JI Bing, FENG Linxian. STUDY ON THE PREPARATION OF HIGH MOLECULAR WEIGHT POLY(FERROCENYL DIMETHYLSILANE) THROUGH THERMAL RING OPENING POLYMERIZATION AND POLY(FERROCENYLDIMETHYLSILANE)/TCNE CHARGE TRANSFER COMPLEX. [J]. Acta Polymerica Sinica (6):788-790(2000)
DOI：

WANG Li, PAN Jie, JI Bing, FENG Linxian. STUDY ON THE PREPARATION OF HIGH MOLECULAR WEIGHT POLY(FERROCENYL DIMETHYLSILANE) THROUGH THERMAL RING OPENING POLYMERIZATION AND POLY(FERROCENYLDIMETHYLSILANE)/TCNE CHARGE TRANSFER COMPLEX. [J]. Acta Polymerica Sinica (6):788-790(2000) DOI：

摘要

Abstract

Ferrocenediyldimethylsilane monomer has been synthesized.A series of poly(ferrocenyl dimethylsilanes) with different molecular weights have been prepared by thermal ring\|opening polymerization of 1

1′-Ferrocenediyldimethylsilane at different polymerization time. It was found that with increasing polymerization time from 5min to 60min the molecular weights of resultant poly(ferrocenyl dimethylsilanes) increase from Mn=1.7×104 to Mn=1.7×105. The reactions of ferrocene with tetracyanoethylene (TCNE) and the reactions of poly(ferrocenyl dimethylsilanes) with tetracyanoethylene (TCNE) were investigated by ESR. A signal with g≈2 was detected from resultant poly (ferrocenyl dimethylsilane)/TCNE system

which indicates the formation of poly (ferrocenyl dimethylsiliane)/TCNE charge transfer complex.

关键词

热开环聚合二茂铁基聚二甲基硅烷四氰基乙烯电荷转移络合物

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