SYNTHESIS AND CHARACTERIZATION OF NOVEL BIODEGRADABLE BLOCK COPOLYMERS OF 6-METHYL-MORPHOLINDIONE AND CAPROLACTONE

YE Wei-ping; Gu Zhong-wei; YANG Ji-yuan; XU Lin; CHEN Xian-li; HOU Ming-shan

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SYNTHESIS AND CHARACTERIZATION OF NOVEL BIODEGRADABLE BLOCK COPOLYMERS OF 6-METHYL-MORPHOLINDIONE AND CAPROLACTONE

Research Bulletin | 更新时间：2021-03-19

- SYNTHESIS AND CHARACTERIZATION OF NOVEL BIODEGRADABLE BLOCK COPOLYMERS OF 6-METHYL-MORPHOLINDIONE AND CAPROLACTONE
- Acta Polymerica Sinica Issue 5, Pages: 609-614(1994)
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- Published：20 October 1994，
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YE Wei-ping, Gu Zhong-wei, YANG Ji-yuan, XU Lin, CHEN Xian-li, HOU Ming-shan. SYNTHESIS AND CHARACTERIZATION OF NOVEL BIODEGRADABLE BLOCK COPOLYMERS OF 6-METHYL-MORPHOLINDIONE AND CAPROLACTONE. [J]. Acta Polymerica Sinica (5):609-614(1994)
DOI：

YE Wei-ping, Gu Zhong-wei, YANG Ji-yuan, XU Lin, CHEN Xian-li, HOU Ming-shan. SYNTHESIS AND CHARACTERIZATION OF NOVEL BIODEGRADABLE BLOCK COPOLYMERS OF 6-METHYL-MORPHOLINDIONE AND CAPROLACTONE. [J]. Acta Polymerica Sinica (5):609-614(1994) DOI：

摘要

Abstract

he block copelymer of 6-- methyl-- morpholinedione and caprolactone have been synthesized based on the stepwise addition of 6 -- methyl -- morpholinedione to the hydroxyl end group of prepolymers using stannous octoate as a catalyst. Themolecular weight of pre-polymer of caprolactone was determined by the molar ratio of caprolactone and 1

4-butanediol. The block structure was confirmed andcharacterized by means of 1H-- NMR

13C-- NMR

and GPC. The thermal analysis were also reported and compared with the random copolymers.

关键词

生物降解6－甲基－25－二酮基－吗啉己内酯嵌段共聚物

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Guangzhou Institute of Chemistry, Chinese Academy of Sciences

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