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Characterization of Polymer Materials by Synchrotron Radiation Hard X-ray Scattering Technology: The Development and Application of
in situ Instruments- ACTA POLYMERICA SINICA Vol. 52, Issue 12, Pages: 1632-1646(2021)
- 作者机构：
1.中国科学技术大学国家同步辐射实验室 安徽省先进功能高分子薄膜工程实验室 中国科学院软物质化学 重点实验室 合肥 230026
2.西南科技大学核废料处理与环境安全国家协同创新中心 绵阳 621010
- 作者简介：
- 基金信息：
DOI：10.11777/j.issn1000-3304.2021.21111
CLC：Published：20 December 2021，
Published Online：20 August 2021，
Received：19 April 2021，
Revised：21 May 2021，
扫 描 看 全 文
赵景云,昱万程,陈威等.同步辐射硬X射线散射表征高分子材料：原位装置的研制和应用[J].高分子学报,2021,52(12):1632-1646.
Zhao Jing-yun,Yu Wan-cheng,Chen Wei,et al.Characterization of Polymer Materials by Synchrotron Radiation Hard X-ray Scattering Technology: The Development and Application of in situ Instruments[J].ACTA POLYMERICA SINICA,2021,52(12):1632-1646.
赵景云,昱万程,陈威等.同步辐射硬X射线散射表征高分子材料：原位装置的研制和应用[J].高分子学报,2021,52(12):1632-1646. DOI： 10.11777/j.issn1000-3304.2021.21111.
Zhao Jing-yun,Yu Wan-cheng,Chen Wei,et al.Characterization of Polymer Materials by Synchrotron Radiation Hard X-ray Scattering Technology: The Development and Application of in situ Instruments[J].ACTA POLYMERICA SINICA,2021,52(12):1632-1646. DOI： 10.11777/j.issn1000-3304.2021.21111.
摘要
同步辐射硬X射线散射技术是表征高分子材料晶体结构和其他有序结构的有力手段. 高时空分辨的现代同步辐射光源具备强大的实时、原位、动态和无损表征能力，在高分子材料加工和服役过程中远离平衡态的多尺度结构演变研究方面有着巨大优势. 为了充分发挥这一优势，合理设计同步辐射原位研究装置，实现原位实验过程中的样品环境控制十分关键. 本文通过结合具体的研究案例，首先介绍同步辐射原位实验的设计、原位研究装置的研制、操作技巧和数据处理等整个在线实验流程，帮助读者建立对同步辐射原位实验的基本认识. 最后，选择了若干具有代表性的高分子材料体系和样品环境，简要概述同步辐射硬X射线散射技术在表征复杂加工外场作用下高分子材料多尺度结构演变方面的应用，帮助读者加深对同步辐射原位研究装置及相关实验过程的理解，以期引发读者的思考，积极拓展同步辐射硬X射线散射技术在高分子材料表征中的应用.
Abstract
The synchrotron radiation hard X-ray scattering technology is a powerful tool to characterize the crystalline and other ordered structures of polymer materials. For the high temporal and spatial resolutions
modern synchrotron radiation light sources own the powerful capability of real-time
in situ
dynamic and non-destructive characterization. Thus
it gives the synchrotron radiation hard X-ray scattering technology a huge advantage for the study of structural evolutions far away from the equilibrium during the processing and service of polymer materials. To give full play to this advantage
the reasonable design of
in situ
instruments and the control of sample environments during the
in situ
synchrotron radiation experiments are critical. In this review
we first introduce the whole procedures of
in situ
experiments through a specific research case
including the design of
in situ
synchrotron radiation experiments
the development of
in situ
instruments
operation skills and data processing. We hope that the detailed introduction can help the audiences establish a fundamental cognition of the
in situ
synchrotron radiation experiments. Finally
we select several representative polymer material systems and the corresponding sample environments
and briefly overview the applications of the synchrotron radiation hard X-ray scattering technology in studying the multi-scale structural evolutions of these polymers under complex processing fields. We believe that these applications would inspire the audiences to think and deepen their understanding on the synchrotron radiation
in situ
experiments by using
in situ
instruments. Undoubtedly
it is beneficial to further expand the applications of the synchrotron radiation hard X-ray scattering technology on the characterization of polymer materials.
关键词
同步辐射硬X射线散射技术同步辐射原位研究装置高分子材料加工多尺度结构演变
Keywords
Synchrotron radiation hard X-ray scattering technologyIn situ instrumentsProcessing of polymer materialsMulti-scale structural evolutions
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