8-羟基喹啉丙烯酸活性酯的合成及其聚合物与蛋白质的偶联

李福绵; 王林; 李跃青; 冯新德

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8-羟基喹啉丙烯酸活性酯的合成及其聚合物与蛋白质的偶联

研究简报 | 更新时间：2021-03-19

- 8-羟基喹啉丙烯酸活性酯的合成及其聚合物与蛋白质的偶联
- SYNTHESIS OF ACTIVE ACRYLIC ESTERS OF 8-HYDROXYQUINOLINE AND CONJUGATION OF PROTEIN WITH THEIR POLYMERS
- 高分子学报 1986年第1期页码：75-79
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- 纸质出版日期：1986-2-20，
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李福绵, 王林, 李跃青, 冯新德. 8-羟基喹啉丙烯酸活性酯的合成及其聚合物与蛋白质的偶联[J]. 高分子学报, 1986,(1):75-79.

LI Fu-mian, WANG Lin, LI Yuio-qin, FENG Xin-de. SYNTHESIS OF ACTIVE ACRYLIC ESTERS OF 8-HYDROXYQUINOLINE AND CONJUGATION OF PROTEIN WITH THEIR POLYMERS[J]. Acta Polymerica Sinica, 1986,(1):75-79.
李福绵, 王林, 李跃青, 冯新德. 8-羟基喹啉丙烯酸活性酯的合成及其聚合物与蛋白质的偶联[J]. 高分子学报, 1986,(1):75-79. DOI：

LI Fu-mian, WANG Lin, LI Yuio-qin, FENG Xin-de. SYNTHESIS OF ACTIVE ACRYLIC ESTERS OF 8-HYDROXYQUINOLINE AND CONJUGATION OF PROTEIN WITH THEIR POLYMERS[J]. Acta Polymerica Sinica, 1986,(1):75-79. DOI：

摘要

Abstract

Active acrylic esters of 8-hydroxyquinoline

8-acryloxy-quinoline (AQ) and 8-me-thacryloxy-quinoline (MAQ) were synthesized from 8-hydroxyquinoline and corresponding acryl chlorides and polymerized. These two polymers

due to the neighbouring group effect of nitrogen atom on the quinolyl ring

are reactive towards ammonolysis or alcoholysis reactions under mild condition and therefore

can be used to couple proteins. Stirring p(AQ) or p(MAQ) with glucoamylase in borate buffer of pH 7 at room temperature

immolbilized enzyme with specific activity of 5328μ/g and 4320μ/g were obtained respectively.

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