基于可逆共价化学的交联聚合物加工成型研究— 聚合物工程发展的新挑战

张泽平; 容敏智; 章明秋

doi:10.11777/j.issn1000-3304.2018.18060

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基于可逆共价化学的交联聚合物加工成型研究— 聚合物工程发展的新挑战

综述 | 更新时间：2021-01-26

- 基于可逆共价化学的交联聚合物加工成型研究— 聚合物工程发展的新挑战
- Research Progress of Processing of Crosslinked Polymers Based on Reversible Covalent Chemistry: a New Challenge to the Development of Polymer Engineering
- 高分子学报 2018年0卷第7期页码：829-852
- 作者机构：
  
  中山大学化学学院聚合物复合材料及功能材料教育部重点实验室　广州 510275
- 作者简介：
  
  E-mail: cesrmz@mail.sysu.edu.cn Min-zhi Rong, E-mail: cesrmz@mail.sysu.edu.cn
  E-mail: ceszmq@mail.sysu.edu.cn E-mail: ceszmq@mail.sysu.edu.cn
- 基金信息：
  
  国家自然科学基金(基金号 51333008, 51603235和51773229)资助项目()
- DOI：10.11777/j.issn1000-3304.2018.18060
  中图分类号：
- 纸质出版日期：2018-7，
  
  收稿日期：2018-2-12，
  
  修回日期：2018-3-7，
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张泽平, 容敏智, 章明秋. 基于可逆共价化学的交联聚合物加工成型研究— 聚合物工程发展的新挑战[J]. 高分子学报, 2018,0(7):829-852.

Ze-ping Zhang, Min-zhi Rong, Ming-qiu Zhang. Research Progress of Processing of Crosslinked Polymers Based on Reversible Covalent Chemistry: a New Challenge to the Development of Polymer Engineering[J]. Acta Polymerica Sinica, 2018,0(7):829-852.
张泽平, 容敏智, 章明秋. 基于可逆共价化学的交联聚合物加工成型研究— 聚合物工程发展的新挑战[J]. 高分子学报, 2018,0(7):829-852. DOI： 10.11777/j.issn1000-3304.2018.18060.

Ze-ping Zhang, Min-zhi Rong, Ming-qiu Zhang. Research Progress of Processing of Crosslinked Polymers Based on Reversible Covalent Chemistry: a New Challenge to the Development of Polymer Engineering[J]. Acta Polymerica Sinica, 2018,0(7):829-852. DOI： 10.11777/j.issn1000-3304.2018.18060.

摘要

可逆共价聚合物能够通过外界刺激(包括加热、光和pH)触发可逆反应，从而实现聚合物拓扑结构的重组，同时在撤销刺激后又可以像不可逆共价聚合物一样保持结构稳定性. 近年来，越来越多的研究者致力于利用该特性来解决交联聚合物加工成型的难题，这不仅打破了传统热塑性聚合物和热固性聚合物的严格界限，而且带来了新的材料研发方法和功能，使得聚合物制品种类更加多样化，其生命周期也相应得以延长. 孕育着传统聚合物工程领域的新突破，具有重要价值. 为及时反映这一态势，本文总结了可逆共价化学的基本原理，阐述了可逆共价聚合物的流变特性，并且综述了由此衍生的含可逆共价键交联聚合物各类成型加工技术原型和应用，如力学性能调控、塑性变形、焊接、纳米填料的分散与增强效应、模压成型与固相回收、注射成型、挤出成型、3D打印、碳纤维复合材料的可控降解与再生等，在此基础上，进一步分析了该新兴领域的挑战和发展趋势.

Abstract

Reversible covalent polymers are able to reorganize their topological structures

via

reversible reactions triggered by external stimuli (including heating

light and pH)

while retaining the stability of irreversible covalent polymers in the absence of the stimuli. Because the transformation only deals with polymerized materials and can be conducted mostly in solid state in the absence of solvents

environmentally friendly and energy saving measures

like self-healing that autonomously repairs damages created during fabrication or usage

have been proposed. In the meantime

many researchers are also devoted to using this feature for solving processing problems of crosslinked polymers. It not only breaks through the strict limits of traditional thermoplastic and thermosetting polymers

but also brings in new methods and new functionalities. As a result

material diversification with extended life cycles becomes available. A series of novel prototype techniques specified for the crosslinked polymers containing reversible covalent bonds are developed accordingly

which include mechanical properties regulation

plastic deformation

welding

dispersion of nano-fillers and their reinforcement effect

compression molding

injection molding

extrusion molding

3D printing

controllable degradation and reprocessing of carbon fibre reinforced composites. Quite a few engineering processes that cannot be realized by means of existing industrial methods come true. Clearly

the research achievements in this area represent possible advancement of classic polymer engineering. In this review

basis of reversible covalent chemistry and rheology of reversible covalent polymer are comprehensively elucidated and analysed

followed by summarizing the applications of above prototype techniques on the basis of the types of the reversible reactions involved (

i.e.

general reversible reactions and dynamic reversible reactions). Moreover

the challenges and development trend of this emerging field are also outlined. On the whole

the innovative knowledge paths are managed to be introduced in a systematic way. It is hoped that more and more scientists will be attracted and join in this promising research.

关键词

可逆共价化学可逆共价聚合物聚合物工程加工成型

Keywords

Reversible covalent chemistryReversible covalent polymersPolymer engineeringProcessingMolding

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