Applications of Quartz Crystal Microbalance in Polymer Studies

Hai-yang Yuan; Chun-feng Ma; Guang-ming Liu; Guang-zhao Zhang

doi:10.11777/j.issn1000-3304.2020.20248

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Applications of Quartz Crystal Microbalance in Polymer Studies

Review | 更新时间：2024-02-20

- Applications of Quartz Crystal Microbalance in Polymer Studies
- ACTA POLYMERICA SINICA Vol. 52, Issue 7, Pages: 806-821(2021)
- 作者机构：
  
  1.中国科学技术大学化学物理系合肥微尺度物质科学国家研究中心安徽省教育厅表界面化学与能源催化重点实验室　合肥 230026
  2.华南理工大学材料科学与工程学院　广州 510640
- 作者简介：
- 基金信息：
- DOI：10.11777/j.issn1000-3304.2020.20248
  CLC：
- Published：20 July 2021，
  
  Published Online：26 January 2021，
  
  Received：13 November 2020，
  
  Revised：04 December 2020，
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袁海洋,马春风,刘光明等.石英晶体微天平在高分子研究中的应用[J].高分子学报,2021,52(07):806-821.

Yuan Hai-yang,Ma Chun-feng,Liu Guang-ming,et al.Applications of Quartz Crystal Microbalance in Polymer Studies[J].ACTA POLYMERICA SINICA,2021,52(07):806-821.
袁海洋,马春风,刘光明等.石英晶体微天平在高分子研究中的应用[J].高分子学报,2021,52(07):806-821. DOI： 10.11777/j.issn1000-3304.2020.20248.

Yuan Hai-yang,Ma Chun-feng,Liu Guang-ming,et al.Applications of Quartz Crystal Microbalance in Polymer Studies[J].ACTA POLYMERICA SINICA,2021,52(07):806-821. DOI： 10.11777/j.issn1000-3304.2020.20248.

摘要

石英晶体微天平(QCM)作为一种强有力的表征工具已被广泛应用于高分子研究之中. 本文中，作者介绍了QCM的发展简史、基本原理以及实验样品制备方法. 在此基础上，介绍了如何基于带有耗散测量功能的石英晶体微天平(QCM-D)及相关联用技术研究界面接枝高分子构象行为、高分子的离子效应以及高分子海洋防污材料，展示了QCM-D技术在高分子研究中的广阔应用前景. QCM-D可同时检测界面高分子薄膜的质量变化和刚性变化，从而反映其结构变化. 与光谱型椭偏仪联用后，还可同步获取界面高分子薄膜的厚度变化等信息，可以有效解决相关高分子研究中的问题. 希望本文能够对如何利用QCM-D技术开展高分子研究起到一定的启示作用，使这一表征技术能够为高分子研究解决更多问题.

Abstract

In this review

the authors introduce the brief history

basic principles

sample preparation

and applications of quartz crystal microbalance (QCM). With the development of QCM technique

the quartz crystal microbalance with dissipation (QCM-D) has been employed to carry out the studies in a wide range of fields of polymer films because it can simultaneously obtain the information on the changes in mass and stiffness of polymer films. Moreover

the combined QCM-D and spectroscopic ellipsometry (QCM-D/SE) technique can be used to further obtain the thickness change and other information of polymer films. To demonstrate the applications of QCM-D in polymer studies

this review presents how the QCM-D and QCM-D/SE can be used to study the conformational behaviors of polymers grafted at interfaces

the ionic effects on polymers

and the polymeric marine antifouling materials. Specifically

(i) QCM-D can be used to study both the conformational behaviors of grafted polymers during the pancake-to-brush and mushroom-to-brush transitions and the stimuli-responsive behaviors of grafted polymers with temperature

and salt concentration as the external stimuli; (ii) QCM-D/SE can be applied to study the ionic effects on polyelectrolyte brushes including specific ion effects

ionic hydrogen bond effects

and ionic hydrophilicity/hydrophobicity effects. The relevant studies can not only clarify the mechanisms of the ionic effects on polyelectrolyte brushes

but also demonstrate that the properties of polyelectrolyte brushes can be tuned with these ionic effects; (iii) QCM-D can be employed to evaluate the performance of polymeric marine antifouling materials

providing a method to screen the materials in laboratory

saving much time and money for marine field tests. The authors hope that this review can provide an inspiration on how to apply QCM-D to carry out polymer studies

enabling this technique to solve more problems in the field of polymers.

关键词

石英晶体微天平高分子刷聚电解质离子效应海洋防污材料

Keywords

Quartz crystal microbalancePolymer brushesPolyelectrolytesIonic effectsMarine antifouling materials

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