In order to improve the redisperisibility of nanocrystalline cellulose(NCC)particles
three grafted reactions with acetylation
hydroxyethylation and hydroxypropylation
respectively were introduced to modify the NCC particle surface.The most advantages of these three methods were that the reaction condition was simple and was easily controlled
while the redispersibility of the resulting products was improved distinctly at the same time.The properties of the modified NCC were characterized by FT-IR
13C-NMR
TEM and TGA.The results showed that the products of the modified NCC
after desiccation
could be dispersed again in the proper solvents to form stable suspensions by ultrasonic treatments
and the diameter of the modified NCC particles did not increase clearly. However
their thermal behaviors were different.The beginning decomposition temperature of the products that NCC was surface modified via hydroxyethylation or hydroxypropylation
respectively
was distinctly lower than that of NCC via acetylation