全息聚合物分散液晶的结构调控与性能

倪名立; 彭海炎; 解孝林

doi:10.11777/j.issn1000-3304.2017.17120

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全息聚合物分散液晶的结构调控与性能

专论 | 更新时间：2021-01-26

- 全息聚合物分散液晶的结构调控与性能
- Structure Regulation and Performance of Holographic Polymer Dispersed Liquid Crystals
- 高分子学报 2017年第10期页码：1557-1573
- 作者机构：
  
  华中科技大学化学与化工学院能量转换与存储材料化学教育部重点实验室武汉 430074
- 作者简介：
  
  [ "彭海炎，男，1984年8月生，华中科技大学化学与化工学院副教授. 2008年华中科技大学化学与化工学院应用化学专业本科毕业，保送该校直攻博研究生，师从解孝林教授和危岩教授，2014年高分子化学与物理专业博士毕业. 2012 ~ 2014年间受国家留学基金委公派赴美国科罗拉多大学波尔德分校联合培养16个月，师从Christopher Bowman教授. 2014 ~ 2015年任广州中国科学院先进技术研究所助理研究员，2015 ~ 2016年在香港城市大学Robert Li教授课题组从事博士后研究. 2014年获第八届中国流变学青年奖，2015年获湖北省优秀博士学位论文.目前主要从事光聚合反应机理、动力学、流变学以及全息光聚合物复合材料研究" ]
  [ "解孝林，男，1965年9月生，华中科技大学化学与化工学院教授. 1987年武汉化工学院化工系本科毕业，1990年成都科技大学高分子材料专业硕士研究生毕业，1995年获四川大学工学博士学位，1997年12月浙江大学博士后出站并加盟华中科技大学工作.曾赴香港城市大学、香港理工大学进行合作研究，澳大利亚悉尼大学和美国科罗拉多大学波尔德分校访问教授. 2005年获湖北省五四青年奖章，2008年获国家杰出青年科学基金，2010年获国家自然科学二等奖(排名第一)，2015年入选科技部创新人才推进计划重点领域创新团队负责人.目前主要从事激光全息高分子、聚合物基电子封装材料和低成本高性能可降解高分子材料的研究" ]
- 基金信息：
  
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- DOI：10.11777/j.issn1000-3304.2017.17120
  中图分类号：
- 纸质出版日期：2017-10，
  
  收稿日期：2017-5-2，
  
  修回日期：2017-5-27，
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倪名立, 彭海炎, 解孝林. 全息聚合物分散液晶的结构调控与性能[J]. 高分子学报, 2017,(10):1557-1573.

Ni Ming-li, Peng Hai-yan, Xie Xiao-lin. Structure Regulation and Performance of Holographic Polymer Dispersed Liquid Crystals[J]. Acta Polymerica Sinica, 2017,(10):1557-1573.
倪名立, 彭海炎, 解孝林. 全息聚合物分散液晶的结构调控与性能[J]. 高分子学报, 2017,(10):1557-1573. DOI： 10.11777/j.issn1000-3304.2017.17120.

Ni Ming-li, Peng Hai-yan, Xie Xiao-lin. Structure Regulation and Performance of Holographic Polymer Dispersed Liquid Crystals[J]. Acta Polymerica Sinica, 2017,(10):1557-1573. DOI： 10.11777/j.issn1000-3304.2017.17120.

摘要

全息聚合物分散液晶（HPDLCs）是由富聚合物相与富液晶相周期性排列而成的结构有序高分子复合材料.HPDLCs通过单体/液晶复合体系的光聚合诱导相分离而形成，如何调控并定量化描述复合体系的光聚合反应动力学、凝胶化行为和相分离程度，进而获得结构规整、电光性能优异的HPDLCs是关键难题.专论概述了光引发体系、单体结构、纳米无机材料掺杂对HPDLCs结构及性能的影响.光引发阻聚剂通过引发和阻聚的竞争与协同，降低了光聚合反应速率、延迟了凝胶时间，促进形成衍射效率达90%的HPDLCs.超支化单体降低了复合体系黏度和光聚合反应速率，延迟了凝胶时间，促使形成衍射效率达94%、具有一维光子晶体结构的HPDLCs.丙烯酰胺单体优化了相分离结构，将HPDLCs的衍射效率提升至98%.纳米硫化锌掺杂在保持规整结构和高衍射效率的同时，大幅降低了HPDLCs的驱动电压.研究还确定了HPDLCs的相分离程度与凝胶时间的函数关系.构建兼具高衍射效率与低驱动电压的HPDLCs，推进其在彩色3D图像存储等领域的应用仍是重要课题.

Abstract

Holographic polymer dispersed liquid crystals (HPDLCs) are one type of polymer composites in the form of periodically distributed polymer-rich phase and LCs-rich phase with ordered structure. HPDLCs are typically formed

via

photopolymerization induced phase separation of monomer/LCs mixtures. Despite of the extensive research on HPDLCs since 1993

it remains challenging to tune and quantitatively describe the photopolymerization kinetics

gelation behaviour

and degree of phase separation

for the aim of achieving HPDLCs with predesigned regular structure and desired electro-optical performance. This review summarizes the influence of the photoinitiating system

monomer structure

and doping of inorganic nanomaterials on the structure and performance of HPDLCs. The deployment of photoinitibitor

which held competitive and synergetic photoinitiation and photoinhibition functions

was found to be able not only to trigger the photopolymerization upon laser light exposure

but also to decrease the photopolymerization rate

to delay the gelation

thus helping the formation of HPDLCs with a high diffraction efficiency of 90%. The first photoinitibitor was composed of 3

3'-carbonylbis(7-diethylaminocoumarin) (KCD) and a co-initiator

-phenylglycine (NPG). The photoinitiation and photoinhibition functions were also noted later in a normally used photoinitiating system composed of rose bengal (RB) and

-phenylglycine (NPG). Hyperbranched monomer was disclosed to be able to decrease the mixture viscosity and the reaction rate

and also to delay the gelation. Consequently

HPDLCs with a diffraction efficiency of 94% and one-dimensional photonic structure were afforded on the basis of the employment of hyperbranched monomer because of the enhanced phase separation. Acrylamide monomer was found to optimize the phase separated structure

offering HPDLCs with a high diffraction efficiency of up to 98%. The doping of mercaptoethanol functionalized nano-ZnS was found to decrease dramatically the driving voltage while maintaining regular structure and high diffraction efficiency of HPDLCs. These ZnS nanoparticles were expected to be localized in the polymer rich-region to increase the conductivity of the region. The numerical relationship between the degree of phase separation of HPDLCs and gelation time of monomer/LCs mixtures is also highlighted. We believe that there remain opportunities to increase simultaneously the diffraction efficiency while decreasing the driving voltage of HPDLCs. Colored 3D holographic image storage and other practical applications of HPDLCs should be further advanced.

关键词

聚合物分散液晶全息光聚合相分离图像存储

Keywords

Polymer dispersed liquid crystalsHolographyPhotopolymerizationPhase separationImage storage

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